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Indirect spectrophotometric determination of capsaicinoids in Capsicum peppers using the reaction of complex Co(II) with 4-(2-pyridylazo) resorcinol.

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Academic year: 2017

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Figura 2. Espectros das misturas CAPS+PAR+Co(II) em tampão borato pH  8,35, sendo C PAR  = 2,5×10 -5  mol L -1 , C Co(II)  = 1,25×10 -5  mol L -1  e V CAPS  = 0, 0,5,  1, 2,5, 5 e 7,5 mL de extrato de pimenta dedo de moça diluído no tampão de  trabalho na
Figura 3. Espectros das misturas de C PAR  = 2,5×10 -5  mol L -1 , C Co(II)  = 1,25×10 -5  mol L -1  e C CAPS  = 14,35 mg L -1
Tabela 1. Dados de espectros de massas (MS/MS) de amostras contendo CAPS
Figura 7. Cromatogramas do padrão de DHCAP 0,5 mg mL -1 , extrato de  pimenta dedo de moça (DM)
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