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J. Braz. Chem. Soc. vol.20 número10

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Figure 2. Plots of i p  versus pH (curve a) and δi p  / δpH versus pH (curve b)  of 1.0×10 -4  mol L -1  gatiloxacin in B-R universal buffer of various pH  values at a scan rate of 100 mVs -1 .
Figure 4. Cyclic voltammograms of 5.0×10 -7  mol L -1  bulk gatiloxacin  in a B-R universal buffer of pH 7.0 at a scan rate of 100 mVs -1  recorded  following preconcentration by adsorptive accumulation onto the HMDE  at open circuit conditions (a) and the
Table  1.  Characteristics  of  the  calibration  curves  of  SW-AdCS  voltammetric  determination  of  bulk  gatiloxacin  in  a  B-R  universal  buffer  of  pH  7;
Figure 6. SW-AdCS voltammograms of 5.0 ×10 -7  mol L -1  gatiloxacin  during induced degradation in 2.5 mol L -1  HCl for different time intervals  t : (a) 0, (b) 90, (c) 180, and (d) 360 min; pH 7, t acc  = 30 (Dotted line is  the background)
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