Cateto, C.A., Naceur, M.N., Rodrigues, A
.
E., Barreiro, M.F., "Lignin characterization
by
acetylation procedures",
9th International Chemical Engineering Conference - CHEMPOR
2005, Coimbra, Portugal, 21-23 September {2005) (poster)
CHEMPOR 2005
Coimbra-
21
51-23rd
September
2005
PROGRAMME
Wednesday
21
stSeptember
18:00-19:30 Welcoming participants
Thursday
22"d
September
08:30-09:00 Welcoming participants
09:00-09:30 Opening Session
Session 1
Chairpersons:
F. Ramoa Ribeiro
and
Lelio
Quaresma
Lobo
09:30-10:15 Invited Lecture: Dr.Trevor Evans (Chief Executive& Secretary lchemE);
"The role of National Societies and the European Federation of Chemical Engineering in
promoting a better appreciation of chemical engineering as an essential contributor
to the
quality
of life and to achieving a suitable future."
10:15-11:00 Invited Lecture: Prof. Jens Nielsen (Technical University of Denmark)
"The role of chemical engineering in modern biotechnology.
"
11 :00-11:15
Coffee Break
,~1 I ,.--~.r:-~!·~-;: I • • ' ' ' - I • • f•; .. -. . . - • I : ;
Session 2
Chairpersons:
Moura Bordado
and
Salvador Pinheiro
11:20-12:05 Invited Lecture Eng° C
.
Pedro Nunes (CUF)
Uma Perspectiva Estrategica da Industria da Refinac;ao de Petroleos
e
Petroquimica em
Portugal.
Chairpersons:
Moura Bordado
and
Salvador Pinheiro
12:05-12:25 IP006- Methylacetylene and Propadiene Reactors Optimization in the Sines Repsol Steam
Cracker Plant
Andre A.Vilelas, Jose P. Braga
Interface Team, Olefins Plant, Repsol Steam Cracker,Sines, Portugal.
12:25-12:45 IP034- Study and optimization of a hydrogen distribution network: refinery case study
Andre Fonseca, Vitor Sa, Hugo Bento, Manuel L.C. Tavares, Lufsa A.C.N. Games Chemical Engineering Department, Institute Superior de Engenharia, I PP, Porta; Technology Area, Galp Energia, 4451-852 Lec;a da Palmeira, Portugal.
12:45-13:05
IP01
0- Separation of branched hexane isomers on zeolite BETA
Patrick S. Barcia, Jose A. C. Silva, AHrio E. Rodrigues
Escola Superior de Tecnologia e Gestae, Institute Politecnico de Braganc;a;
Laboratory of Separation and Reaction Engineering, Departamento de Engenharia Quimica, FEUPorto.
13:05-13:25 IP068- Recuperac;;ao do ciclohexanol e da ciclohexanona do processo de produc;;ao de
anilina
Fernando P. Mendes, Marco A. F. Prior, Rui M. F. Andrade, Susana C. G. Caldas, Mario Jorge 0. Pinho, Laura M. T. Santos, Luls M. Castro, Nazare C. Pinheiro, Manuel A. Ramos, Belmiro P. M. Duarte Quimigal S.A., Qufmica de Portugal, Portugal;
Departamento de Engenharia Quimica, Institute Superior de Engenharia de Coimbra.
13:25-13:45 MSC031-Multivariate analysis of the benzene nitration process for pollution prevention
Paulo A. Quadros, Marco S. Reis, Cristina M. S. G. Baptista Chemical
Session 3
Chairpersons:
Alirio Rodrigues
and Rosa
Quinta Ferreira
12:05-12:25 ESF005-Efeito protector da matriz em catalisadores de "cracking" catalitico em relac;;ao ao
envenenamento por bases azotadas
G. Caeiro, Patrick Magnoux, J.M. Lopes e F. Ramoa Ribeiro
CEBQ, Institute Superior Tecnico, Lisboa ; Lab. de Catalyse en Chimie Organique, Poitiers, France
12:25-12:45 ESF021- Degradac;;ao fotocatalitica de corantes texteis
Edilberto T. Scares, Marla A. Lansarin, Celso C. Moro, Cristina L. Souza e Natalia Klafke
16
:
25-16:45 ESF051- Effect of hydrodynamic conditions in osmotic evaporation using membrane
contactors
V. D. Alves, I. M. Coelhoso
REQUIMTE I CQFB, Faculdade de Cilmcias e Tecnologia, Universidade Nova de Lisboa.
Chairpersons:
Ana Pau/a P6voa and Adelio Mendes
16:05-16:25 QL082-Protein recovery from tannery wastewater containing chromium by nitrogen
removal
Francisco N.S. Basilic, Helder F. C. Marques, Marta I.G. Sousa, Raquel A.P. Silva, Nfdia S. Caetano
Chemical Engineering Department, Institute Superior de Engenharia do Porta;
LEPAE, Chemical Engineering Department, Institute Superior de Engenharia do Porta.
16
:2
5
-
16
:
45 QL 111-Preparatlon of Therapeutic Contact Lenses Using Supercritical and Compressed
Fluids
Hermfnio C. de Sousa, Ana Rita C. Duarte, Joana P. Guerra, Viviana P. Costa, Eugenic O.B. Leite, Catarina
M.M. Duarte, Maria H. Gil
Departamento de Engenharia Qufmica, Faculdade de CiE'mcias e Tecnologia, Universidade de Coimbra;
Institute de Biologia Experimental e Tecnol6gica, Oeiras;
Faculdade de Ciencias da Saude, Universidade da Beira Interior, Covilha.
Session 17
Chairpersons:
Ant6nio Portugal
16:05-16:25 QL 115-Life Cycle Assessment of bioethanol from sugar beet and wheat- comparison with
gasoline
Joao Malya, Fausto Freire
Mechanical Engineering Department, ISEC, Coimbra Polytechnic Institute;
Mechanical Engineering Department, Faculty of Sciences and Technology, University of Coimbra.
16
:
25
-
16
:
45 QL090-The emergence of a new field of application of chemical and systems engineering
principles: pharmaceutical engineering
Jose Cardoso de Menezes
Centre for Chemical & Biological Engineering, 1ST, Technical University of Lisbon.
16
:
45-17
:
00
Coffee Break
.· 1-l~.L·•,-~ .
·J
·
· .
· ·
j
'
.
...
Session 18
Chairpersons:
Sebastiao Feyo de Azevedo
and
Pedro Saraiva
17
:
00-17
:
40 Chemical Engineering Education- Prof
.
Robert
Armstrong,
M IT, USA
"Frontiers in
Chemical Eng
i
neer
in
g
Education."
17
:
40-18
:
40 Forum Chemical Engineering Education
18
:
40-19
:
00 Closing Session
POSTER SESSIONS
Thursday 22"d
September
• r ~, ... ii~Lrt~
...
~ :~-,. .::
~'•' J .. ; • ,I l , ~ ~· ·, \ ' t • . , r-. ... ~ - - - .... ':1 - < <..._.; l ~ • ... • • • ' • ' •
1
ESF-Engineering Sciences and Fundamentals
ESF001
-
Mass transfer to clean bubbles at low turbulent energy dissipation
Sebastiao S. Alves, Jorge M. T. Vasconcelos, Sandra P. Orvalho,
Centra de Eng. Biol6gica e Qufmica, Dept. of Chemical Engineering, Institute Superior Tecnico, Lisboa, Portugal.
ESF003- Plug Formation and Flow Regimes
in
Dense-Phase Pneumatic Conveying
Fernando A. V. Silvano, Severino S. Pandiella
Departamento de Engenharia Mecimica, Escola Superior de Tecnologia e Gestao, Institute Politecnico de Leiria, Leiria,
Portugal.
School of Chemical Engineering and Analytical Science, The University of Manchester, Manchester, U. K.
ESF004
-
Dynamic model of a supercritlcal carbon dioxide heat exchanger
Joao B. Fernandes, Pedro C. Simoes, Jose Paulo Mota
REQUIMTE, Chemistry Department, University Nova of Lisbon, Quinta da Torre, Caparica, Portugal.
ESF
006
-
Safety study for scaleup of dehydroabietic
acid
Carlos Lopes, Carla Raminhos, Joao A.A. Lourenyo
LEPAE - Departamento de Engenharia Qufmica, Faculdade de Engenharia, Universidade do Porta, Porto, Portugal.
IP016 -Novas materiais de
eh~ctrododo tipo espinela para a degradac;ao electroquimica do clorof6rmio
Sandra Ferreira, M. Helena Mendont;:a, M. Rosa Nunes, M. I. da Silva Pereira, Femanda Costa, J. M. Nogueira
Departamento de Qufmica e Bioqufmica, Centra de Ciencias Moleculares e Materiais, Faculdade de
Cilmcias, Universidade de Lisboa, Lisboa, Portugal.
IP018
-Estudo
comparative da extrac;ao do acido clavulfmico por solvente organico e sistemas de duas
fases aquosas
Luciana Machado Brites, Daniela Bataglia Hirata, Marlei Barboza Pasotto, Caries Osamu Hokka
Departamento de Engenharia Qulmica, Universidade Federal de Sac Caries, Sac Caries, SP, Brasil.
IP019 -Validac;ao de modelo te6rico para a purificac;ao de acido clavulanico em resina polimerica de
troca ionica.
Marina T.A.G.Mendes, Marlei Barboza Pasotto, Wu Hong Kwong, Carlos Osamu Hokka
Departamento de Engenharia Qufmica, Universidade Federal de Sac Carlos, Sac Caries, SP, Brasil.
IP021 -Impact of lignin quality (h/g ratio) in kraft pulping of Maritime pine
Ana Alves, Helena Pereira, Denilson da Silva Peres, Guillaume Chantre and Jose Rodrigues
Centra de Estudos Florestais, Institute Superior de Agronomia, Universidade Tecnica de Lisboa, Lisboa, Portugal;
Institute de lnvestigat;:ao Cientrfica Tropical, Centre de Estudos de Tecnologia Florestal, Lisboa, Portugal;
Laboratoire Bois Process, Afocel, Domaine de I'Etant;:on, Nangis, France.
IP022 -Giant reed- an alternative raw-material for papermaking
Sandra Abrantes, Maria Emflia Amaral, Ana Paula Costa, and Ana Paula Duarte Unidade de lnvestigat;:ao de Materiais Texteis e Papeleiros;Departamento de Ciencia e Tecnologia do Papel, Universidade da Beira Interior, Covilha, Portugal.
IP023 -Copolymerisation Kinetics of a Divinyl p-tert-Butylcalix[4]arene Derivative and Styrene
determined by FT-IR spectroscopy
Alexandra I. Costa, Patrlcia D. Barata, Jose V. Prata
Sect;:ao de Qulmica Organica, Departamento de Engenharia Qulmica and Centre de lnvestigat;:ao de Engenharia Qufmica e
Biotecnologia, Institute Superior de Engenharia de Lisboa, Institute Politecnico de Lisboa, Lisboa, Portugal.
IP024
=
IP056 -Argilas organofilicas como alternativa para remediac;ao de areas contaminadas por
hidrocarbonetos
Kleberson R. 0. Pereira, Marilda M. G. Ramos Vianna, Meiry G. F. Rodrigues, Francisco R. Valenzuela Diaz
LMPSol, Departamento de Engenharia Metalurgica e de Materiais, Universidade de Sac Paulo, Sao Paulo, SP, Brasil;
LABNOV, Departamento de Engenharia Qulmica, Universidade Federal de Campina Grande, Campina Grande, PB, Brasil.
IP029 -Surface energy, surface area and SEM imaging of eucalyptus globu/us fibres network after
beating, web forming and sizing
Grat;:a V.S. Carvalho, Jose M. R. C. A. Santos, Ant6nio A. Martins, Margarida L. Figueiredo
Chemical Engineering Department, University of Coimbra, Coimbra, Portugal;
Dept. Chem. Tech., Polytec. Inst. of Bragant;:a, Bragant;:a, Portugal;
RAIZ- Forest and Paper Research Institute, Aveiro, Portugal.
IP030 -Substituicao do carbonate de calcio pelo gesso na carga mineral de tubos de pvc
lvania S. Lima, Domingos S. H. MaltaDepartamento do Basico, Escola Politecnica de Pernambuco, Universidade de Pernambuco, Madalena, Recife,
Pernambuco, Brasil;
Departamento de Qulmica, Universidade Cat61ica de Pernambuco, Boa Vista, Recife, Pemambuco, Brasil.
IP031 -Clonal variation and influence of extractives of Eucalyptus globulus Labill. in kraft pulping
Jorge Gominho, Jose Rodrigues and Helena PereiraCentra de Estudos Florestais, Institute Superior de Agronomia, Lisboa, Portugal;
Forestry and Forest Products Group, IICT, Tapada da Ajuda, Lisboa, Portugal.
IP032 -Improvement of HZSM-5 zeolite performance in the transformation of bioethanol into olefins by
alkaline treatment
A. Alonso, B. Valle, A. Atutxa, A.G. Gayubo, A.T. Aguayo
Dpto. lngenierla Qufmica, Universidad del Pals Vasco, Bilbao.
IP033 -Biodiesel- Combustive! Alternative
Pedroso, L.M., Falcao, J., Sim6es, P.N., Simao, A.V., Portugal, A.
Grupo de Computat;:ao, Estatfstica e Materiais (CEM), Departamento de Engenharia Qufmica, Universidade de Coimbra,
Coimbra, Portugal;
Camara Municipal de Coimbra, Coimbra, Portugal.
I
P035 -Lignin characterization by acetylation procedures
Carolina Cateto, Filomena Barreiro, Alfrio Rodrigues
LSRE- Laboratory of Separation and Reaction Engineering;
Escola Superior de Tecnologia e de Gestae, Institute Politecnico de Bragant;:a, Bragant;:a;
Faculdade de Engenharia da Universidade do Porta, Porta.
IP036 -Development of Image Analysis Methods to Evaluate Barley
I
Malt Grain Size
Ant6nio L. Amaral, Orlando Rocha, Cristina Gonyalves, Ant6nio Augusto and Eugenic C. Ferreira
Universidade do Minho, Departamento de Engenharia Biol6gica, Braga, Portugal;
Institute Politecnico de Bragant;:a, Departamento de Tecnologia Qufmica- ESTIG, Bragant;:a, Portugal;
UNICER, Via Norte, Let;:a do Balio, S. Mamede de lnfesta, Portugal.
! " # $ %
$ & # ' ( ) " # *
+& # & &" ," # # %
& # # ! % " & " - &
. " # & % " " % - & & & & " /
& - 0 & ! " # " % &
# &" ," # 0 # -$ % 0 " % ) - # , !" 1 22 3 0 224 / % & %% # " ## !5 & # # ) ) ! $ & # + & " 6 * " & / 7 % - % % - & # 8 - 9- $% &" % # % % - 0 & # 4::: ;<: = - & # 4 = ! 0 % - " " ! # & . # & % % / # # & %
-& # & ! <:> = ) ! &
% +& ) ! - ## !" & " % 6 * % / ? %& . / * " & . ? ! +& " - ) & % ! !" ? 22 +& ) - @ ;: A - & # B "
!
!
+& !5 ) # & - 0 , & ! " # "%
" % - " &" = %" , & ) " % - " !" +/ 7 % $ ) ,% - @ % C ! % # & " C * # " C 1 " % # & " %
"
"
+& 5 & ! ) & +/ % ) " % @
# & &" ," D'E & ! 4 4 = +&
% !" & # - ! ;4: < : = C ! / & ! " FD & %% # - - # ! > > >;; = C / ! '&" ! 'E ;G =C / # ! ! & ! - : : ;: = & # =E =D # & # 'D= FD = E % +/ % # % @ ! # % # " % : 34 34 .3 1 34 34 .3 1 29 36 .0 2 28 40 .0 7 1684.3 5 15 98 .8 815 11 .8 3 14 64 .7 9 14 21 .5 13 73 .76 12 68 .2 2 12 20 .25 11 43 .4 9 10 81 .251028.5 9 96 1.4 32 85 6.1 27 81 2.8 35 36 40 .5 3 35 20 .6 8 29 40 .64 28 39 .7 5 17 66 .0 4 17 37 .2 5 15 93 .5 31507 .1 5 14 64 .0 8 14 20 .7 8 13 68 .11 12 72 .1 41205.19 10 90 .0 3 103 2.44 96 5.4 99903.234 85 5.2 49 82 6.4 57 4000 3500 3000 2500 2000 1500 1000 Frequence (cm-1) Initial Sample Sample 01 + H ) ! = % ! - - " % # # & - & % : - & " % :G 20 40 60 80 100 4000 3500 3000 2500 2000 1500 1000 Frequência (cm -1) Amostra 01 Amostra 1 Banda de referência Sample 01 Sample 08 Reference vibration + H ) ! = 80 100 + 80 100 + # # $$
!
!
@ % % " " % % & % &'(
)
'(
)
+& " % & % # % " # &
! &" ,"
+ ) & ## ## & ! % B & % !"
# / & - " & ,% % % & !
) " & %# *
*
" - ! &
& /$D 42::@ :: $ #
-- & & % # & " %
# & +& !5 ) - ) # & "
% ! & & ) ! # ## % % &" ," ?* " $ % " " @ *" + % + 1 " : <: : = GG@ E # , ;: ;: A - & : <: : = : : <::: = G: :4 <: 4 = < B " :< <: = : :; <: = 4< :> <::4 = ;: :G <: : >222 GG@ ;: :2 <:: : G:: GG@ : : <: : G:: GG@ G: <::: = G:@ : ;: :::2 = <:@<: + % 4 & 20 40 60 4000 3500 3000 2500 2000 1500 1000 Frequência (cm -1) Amostra inicial Amostra 01 Amostra 02 Amostra 03 Banda de referência Initial sample Sample 01 Sample 02 Sample 03 Reference vibration < ## # & & " " # & % - & " + H ) ! = 20 40 60 4000 3500 3000 2500 2000 1500 1000 Frequência (cm -1) Amostra inicial Amostra 1 Amostra 2 Amostra 3 Banda de referência Initial sample Sample 08 Sample 09 Sample 10 Reference vibration 4 ## # & & " " # & % - & " + H ) ! = +& ! & @ +& " - % # & ! & DE & ) ! 4 :' 4;: I - - " ! ) C
! E & & % # " &
"
+& , " # & - ! # # &
% # " + ! # & " % # # $$ - ! # - ) # 2>8 - 9- " ! *" &" B - % " % " ) 22 <8 / B - ) *" &" - ) ) ! #