Certificado de Ensaio e Análise /2011

Rua Frederico Von Martius, 76

Vila Monumento - São Paulo – SP

CEP 01548-010

A/C: Sr. Hugo Monaco

2.

OBJETIVO:

Determinação das emissões gasosas e consumo de veículos

automotores conforme NBR 6601/2005 e NBR 7024/2010.

3.

DADOS DA AMOSTRA:

01 veículo Toyota Hilux - M/T

Motor: 102 cv - Pneus: 215/80R169

Data do recebimento: 28/11/2011

01 veículo Chevrolet S10 - M/T

Motor: 140 cv - Pneus: 225/75R15

Data do recebimento: 05/12/2011

01 veículo Volkswagen Amarok - M/T

Motor: 122 cv - Pneus: 205R16c

Data do recebimento: 12/12/2011

Para informações complementares, vide relatório de ensaio.

4.

DATA DE EMISSÃO:

12/01/2012

Os resultados deste Relatório se referem somente aos itens ensaiados/analisados.

5.

PROCEDIMENTO

NBR 6601/2005 - Veículos rodoviários automotores leves - Determinação de hidrocarbonetos, monóxido de

carbono, óxidos de nitrogênio, dióxido de carbono e material particulado no gás de escapamento;

NBR 7024/2010 - Veículos rodoviários automotores leves - Medição do consumo de combustível - Método de

ensaio, conforme item 6.3 Cálculo do consumo pelo método por balanço de carbono;

Resolução Nº 40, DE 24.12.2008 – DOU 26.12.2008 – Agência Nacional do Petróleo, Gás Natural e

Biocombustíveis;

6.

DADOS DO COMBUSTÍVEL

Diesel Padrão de Referência

Massa específica 0,8308 kg/l, a 20°C

Ensaios: 8389 ; 8453 e 8537

Diesel Padrão de Referência

REPRODUÇÕES DESTE DOCUMENTO SÓ TÊM VALIDADE SE FOREM INTEGRAIS E AUTORIZADAS PELO LACTEC

DOC LEME - 31 Data: AGO/2010 Revisão: 05

Dinamômetro elétrico Horiba LDD 48’’ – 86 monorolo;

Analisadores: Horiba 7200 H (CO, HC, NOx, CO2, CH4) E 7500 H (CO, HC, Nox, CO2, O2);

Amostrador: CVS - CFV Horiba modelo CVS - DPS 88;

Balança de Microgramas CAHN;

8.

CONDIÇÕES DE ENSAIO

O ajuste das forças aplicadas pelo Dinamômetro Horiba de 48’’ foi realizado através da inserção dos tempos de

desaceleração em pista fornecidos pelo cliente:

Toyota Hilux - Motor: 102 cv - M/T

PRR80 (hp): 20,6

Chevrolet S10 - Motor: 140 cv - M/T

PRR80 (hp): 21,4

Volkswagen Amarok - Motor: 122 cv - M/T

PRR80 (hp): 19,6

9.

RESULTADOS E DADOS ADICIONAIS DO ENSAIO DE EMISSÕES

Vide páginas 03 até 14.

9.1 OBSERVAÇÔES

•

Os ensaios nº 8389, 8453 e 8537 foram realizados com combustível Diesel Padrão de referência sem

aditivo

•

Os ensaios nº 8415, 8468 e 8556 utilizou-se o aditivo XP3 na concentração de 1/4000 litros, fornecido

pelo cliente.

Responsável pela análise:

________________________________

Katia Cristine da Silva

Representante da Qualidade

Registro LACTEC 1139

Aprovação:

________________________________

Dennis Rempel

Signatário Autorizado

Registro LACTEC 547

Run Number: 8389 Requester: ECOFUEL

Test Cell: LACTEC LEME Vehicle Type: Hilux_TOYOTA

Test Date: 30/nov/11 Vehicle ID: 84JER32G94028842

Test Start Time: 01:20:51 Transmission: Manual

Test Type: Brazil Cert Odometer: (km) 69717

Operador: RICARDO Inertia Wt: (kg) 2041

Driver: RICARDO Dyno Coeff A: (nt) 255.91

Fuel Type: Diesel_S10_01_11 Dyno Coeff B: (nt/kph) 0.0000

Shift Table 1: 25_40_65_72 Dyno Coeff C: (nt/kph^2) 0.066800

Shift Table 2: EPA505_5spd_25_40_65_72 Dyno hp @ 50 mph: 20.6

Soak Start Date: 29/11/2011 Driver Errors: 0

Soak Start Time: 00:12 Pretest Remarks:

Test Conditions

Phase 1

Phase 2

Phase 3

Phase Start Time: 01:27:33 01:35:59 02:00:40

Test Time (sec): 506.7 866.8 506.4

Avg. CVS Flow Rate (m^3/min) 8.30 8.28 8.27

CVS Volume (m^3 20degC) 70.52 120.27 70.24

Dilution factor: 11.410 18.868 12.791

Bag Analysis Time (sec): 1011.4 272.1 184.8

Driver Out of Limits (sec): 0.0 0.0 0.0

Distance (km) 5.803 6.234 5.817

Crank Time (sec): 1.5 - 1.2

Hold Time (sec): 0.0 0.0 0.0

Avg. Cell Temp (degC) 22.2 22.8 22.3

Avg. Barometer (kPa) 90.83 90.81 90.79

Avg Dew Point (degC) 14.10 14.17 13.98

Avg. Real Humidity (%) 60.0 58.1 59.1

Specific Humidity (gm/kg) 11.20 11.26 11.12

Hum Corr Factor: 1.016 1.018 1.014

Bag Results

THC

CO

NOx

CO2

CH4

Phase 1

(ppm)

(ppm)

(ppm)

(%)

(ppm)

Sample: 12.684 22.829 34.705 1.171 2.039 Ambient: 3.380 0.000 0.059 0.042 1.776 Net Concentration: 9.601 22.829 34.651 1.132 0.419

Phase 2

Sample: 8.397 3.768 15.617 0.709 2.044 Ambient: 3.168 0.000 0.037 0.043 1.774 Net Concentration: 5.397 3.768 15.581 0.669 0.363

Phase 3

Sample: 8.456 6.517 32.667 1.046 1.893 Ambient: 3.276 0.000 0.037 0.042 1.773 Net Concentration: 5.437 6.517 32.633 1.007 0.258

Mass Results (g/ km)/(g)

Phase 1 0.068 0.393 0.323 1.876 0.820 4.757 Phase 2 0.059 0.366 0.085 0.528 0.586 3.655 Phase 3 0.038 0.219 0.092 0.533 0.765 4.449 Weighted (Phase1,2,3) 0.055 0.136 0.684

Mass Results (g/ km)/(g)

Phase 1 252.134 1,463.187 0.003 0.020 0.064 0.374 Phase 2 236.381 1,473.636 0.005 0.029 0.056 0.350 Phase 3 222.802 1,296.058 0.002 0.012 0.036 0.210 Weighted (Phase1,2,3) 235.911 0.004 0.052

Fuel Economy (km/liter)

Phase 1 10.420

Phase 2 11.131

Phase 3 11.812

THC

CO

Nox

REPRODUÇÕES DESTE DOCUMENTO SÓ TÊM VALIDADE SE FOREM INTEGRAIS E AUTORIZADAS PELO LACTEC

DOC LEME - 31 Data: AGO/2010 Revisão: 05

Run Number: 8389 Requester: ECOFUEL

Test Cell: LACTEC LEME Vehicle Type: Hilux_TOYOTA

Test Date: 30/nov/11 Vehicle ID: 84JER32G94028842

Test Start Time: 01:20:51 Transmission: Manual

Test Type: Brazil Cert Odometer: (km) 69717

Operador: RICARDO Inertia Wt: (kg) 2041

Driver: RICARDO Dyno Coeff A: (nt) 255.91

Fuel Type: Diesel_S10_01_11 Dyno Coeff B: (nt/kph) 0.0000

Shift Table 1: 25_40_65_72 Dyno Coeff C: (nt/kph^2) 0.066800

Shift Table 2: EPA505_5spd_25_40_65_72 Dyno hp @ 50 mph: 20.6

Soak Start Date: 29/11/2011 Driver Errors: 0

Soak Start Time: 00:12 Pretest Remarks:

Test Conditions

Phase 1

Phase 2

Phase 3

Phase Start Time(hh:mm:ss): 01:27:33 01:35:59 02:00:40

Particulate Flow Time(sec): 506.7 866.8 506.4

Avg. CVS Flow Rate(m^3/min): 8.30 8.28 8.27

CVS Volume (m^3 20degC): 70.52 120.27 70.24

CVS Dilution factor: 11.410 18.868 12.791

Distance(km): 5.803 6.234 5.817

Crank Time(sec): 1.5 - 1.2

Hold Time(sec): 0.0 0.0 0.0

Avg. Cell Temp.(degC): 22.2 22.8 22.3

Avg. Barometer(kPa): 90.83 90.81 90.79

Avg. Dew Point(degC): 14.10 14.17 13.98

Avg. Specific Humidity(gm/kg): 11.20 11.26 11.12

Avg. Relative Humidity(%): 60.0 58.1 59.1

Particulate Conditions

Avg. Particulate Flow Rate(L/min): 29.7 29.7 29.7

Particulate Volume(L): 251.0 429.6 251.1

Avg. Particulate Temp.(degC): 24.2 24.7 24.9

Avg. Tunnel Temp.(degC): 30.3 31.5 32.0

Sample Particulate Filters

Filter Number

1

2

3

Init. Primary Filter Mass(mg) 71.688 77.720 71.971

Final Primary Filter Mass(mg) 73.366 78.751 73.330

Initial Secondary Filter Mass(mg) 71.622 73.243 56.767

Final Secondary Filter Mass(mg) 71.653 73.252 56.774

Net Combined Filter Mass(mg) 1.6780 1.0310 1.3590

Particulate Results

Filter Mass (g) 0.4710 0.2884 0.3797

Particulate Mass (g/km) 0.0812 0.0463 0.0653

Weighted Particulate Mass

Run Number: 8415 Requester: ECOFUEL

Test Cell: LACTEC LEME Vehicle Type: Hilux_TOYOTA

Test Date: 02-Dec-2011 Vehicle ID: 8AJER32G594028842

Test Start Time: 01:05:29 Transmission: Manual

Test Type: Brazil Cert Odometer: (km) 69746

Operador: CARLOS Inertia Wt: (kg) 2041

Driver: CARLOS Dyno Coeff A: (nt) 255.91

Fuel Type: Diesel_S10_01_11 Dyno Coeff B: (nt/kph) 0.0000

Shift Table 1: 25_40_65_72 Dyno Coeff C: (nt/kph^2) 0.066800

Shift Table 2: EPA505_5spd_25_40_65_72 Dyno hp @ 50 mph: 20.6

Soak Start Date: 01/12/2011 Driver Errors: 0

Soak Start Time: 02:50 Pretest Remarks: Com aditivo

Test Conditions

Phase 1

Phase 2

Phase 3

Phase Start Time: 01:16:06 01:24:32 01:49:04

Test Time (sec): 506.1 866.4 506.2

Avg. CVS Flow Rate (m^3/min) 8.35 8.32 8.31

CVS Volume (m^3 20degC) 70.83 120.80 70.52

Dilution factor: 11.545 19.059 13.088

Bag Analysis Time (sec): 1011.4 272.3 184.8

Driver Out of Limits (sec): 0.0 0.0 0.0

Distance (km) 5.822 6.216 5.774

Crank Time (sec): 1.0 - 1.0

Hold Time (sec): 0.0 0.0 0.0

Avg. Cell Temp (degC) 21.5 22.8 22.0

Avg. Barometer (kPa) 91.12 91.11 91.09

Avg Dew Point (degC) 10.00 10.07 10.00

Avg. Real Humidity (%) 47.8 44.6 46.3

Specific Humidity (gm/kg) 8.48 8.52 8.49

Hum Corr Factor: 0.932 0.933 0.932

Bag Results

THC

CO

NOx

CO2

CH4

Phase 1

(ppm)

(ppm)

(ppm)

(%)

(ppm)

Sample: 14.058 23.330 33.366 1.157 1.986 Ambient: 2.840 0.263 0.037 0.044 1.716 Net Concentration: 11.464 23.089 33.332 1.117 0.418

Phase 2

Sample: 10.053 4.775 15.772 0.702 1.992 Ambient: 2.585 0.176 0.008 0.043 1.708 Net Concentration: 7.604 4.608 15.764 0.661 0.373

Phase 3

Sample: 10.412 7.209 29.352 1.022 1.846 Ambient: 2.703 0.151 0.031 0.043 1.720 Net Concentration: 7.916 7.069 29.324 0.982 0.257

Mass Results (g/ km)/(g)

Phase 1 0.081 0.471 0.327 1.906 0.724 4.214 Phase 2 0.084 0.519 0.104 0.649 0.547 3.403 Phase 3 0.055 0.320 0.101 0.581 0.639 3.691 Weighted (Phase1,2,3) 0.075 0.150 0.609

Mass Results (g/ km)/(g)

Phase 1 249.004 1,449.775 0.003 0.020 0.078 0.452 Phase 2 235.446 1,463.589 0.005 0.030 0.081 0.505 Phase 3 219.824 1,269.233 0.002 0.012 0.054 0.312 Weighted (Phase1,2,3) 233.978 0.004 0.073

Fuel Economy (km/liter)

Phase 1 10.549

Phase 2 11.170

Phase 3 11.968

THC

CO

Nox

REPRODUÇÕES DESTE DOCUMENTO SÓ TÊM VALIDADE SE FOREM INTEGRAIS E AUTORIZADAS PELO LACTEC

DOC LEME - 31 Data: AGO/2010 Revisão: 05

Run Number: 8415 Requester: ECOFUEL

Test Cell: LACTEC LEME Vehicle Type: Hilux_TOYOTA

Test Date: 02-Dec-2011 Vehicle ID: 8AJER32G594028842

Test Start Time: 01:05:29 Transmission: Manual

Test Type: Brazil Cert Odometer: (km) 69746

Operador: CARLOS Inertia Wt: (kg) 2041

Driver: CARLOS Dyno Coeff A: (nt) 255.91

Fuel Type: Diesel_S10_01_11 Dyno Coeff B: (nt/kph) 0.0000

Shift Table 1: 25_40_65_72 Dyno Coeff C: (nt/kph^2) 0.066800

Shift Table 2: EPA505_5spd_25_40_65_72 Dyno hp @ 50 mph: 20.6

Soak Start Date: 01/12/2011 Driver Errors: 0

Soak Start Time: 02:50 Pretest Remarks: Com Aditivo

Test Conditions

Phase 1

Phase 2

Phase 3

Phase Start Time(hh:mm:ss): 01:16:06 01:24:32 01:49:04

Particulate Flow Time(sec): 506.1 866.4 506.2

Avg. CVS Flow Rate(m^3/min): 8.35 8.32 8.31

CVS Volume (m^3 20degC): 70.83 120.80 70.52

CVS Dilution factor: 11.545 19.059 13.088

Distance(km): 5.822 6.216 5.774

Crank Time(sec): 1.0 - 1.0

Hold Time(sec): 0.0 0.0 0.0

Avg. Cell Temp.(degC): 21.5 22.8 22.0

Avg. Barometer(kPa): 91.12 91.11 91.09

Avg. Dew Point(degC): 10.00 10.07 10.00

Avg. Specific Humidity(gm/kg): 8.48 8.53 8.49

Avg. Relative Humidity(%): 47.8 44.6 46.3

Particulate Conditions

Avg. Particulate Flow Rate(L/min): 29.8 29.8 29.7

Particulate Volume(L): 252.0 431.0 251.2

Avg. Particulate Temp.(degC): 23.9 24.6 25.2

Avg. Tunnel Temp.(degC): 29.0 30.7 31.4

Sample Particulate Filters

Filter Number

1

2

3

Init. Primary Filter Mass(mg) 65.950 69.186 67.020

Final Primary Filter Mass(mg) 67.445 70.114 68.310

Initial Secondary Filter Mass(mg) 66.647 67.215 73.577

Final Secondary Filter Mass(mg) 66.664 67.220 73.581

Net Combined Filter Mass(mg) 1.4950 0.9280 1.2900

Particulate Results

Filter Mass (g) 0.4198 0.2598 0.3618

Particulate Mass (g/km) 0.0721 0.0418 0.0627

Weighted Particulate Mass

Run Number: 8453 Requester: ECOFUEL

Test Cell: LACTEC LEME Vehicle Type: S-10

Test Date: 07-Dec-2011 Vehicle ID: 9BG138JJ0B0431489

Test Start Time: 00:17:35 Transmission: Manual

Test Type: Brazil Cert Odometer: (km) 34981

Operador: CARLOS Inertia Wt: (kg) 2041

Driver: CARLOS Dyno Coeff A: (nt) 307.02

Fuel Type: Diesel_S10_01_11 Dyno Coeff B: (nt/kph) 0.0000

Shift Table 1: 15_30_48_70 Dyno Coeff C: (nt/kph^2) 0.062803

Shift Table 2: 3PH_15_30_48_70 Dyno hp @ 50 mph: 21.4

Soak Start Date: 06/12/2011 Driver Errors: 0

Soak Start Time: 06:10 Pretest Remarks:

Test Conditions

Phase 1

Phase 2

Phase 3

Phase Start Time: 00:24:54 00:33:20 00:57:37

Test Time (sec): 506.0 866.7 506.1

Avg. CVS Flow Rate (m^3/min) 8.35 8.31 8.29

CVS Volume (m^3 20degC) 70.80 120.61 70.38

Dilution factor: 11.494 19.423 13.331

Bag Analysis Time (sec): 1953.6 272.2 184.4

Driver Out of Limits (sec): 0.0 0.0 0.0

Distance (km) 5.767 6.164 5.766

Crank Time (sec): 0.9 - 1.0

Hold Time (sec): 0.0 0.0 0.0

Avg. Cell Temp (degC) 22.2 22.4 22.6

Avg. Barometer (kPa) 91.23 91.23 91.22

Avg Dew Point (degC) 14.32 14.26 14.04

Avg. Real Humidity (%) 60.8 60.0 58.5

Specific Humidity (gm/kg) 11.31 11.27 11.11

Hum Corr Factor: 1.020 1.019 1.013

Bag Results

THC

CO

NOx

CO2

CH4

Phase 1

(ppm)

(ppm)

(ppm)

(%)

(ppm)

Sample: 51.014 268.030 79.235 1.134 2.542 Ambient: 3.848 0.000 0.120 0.043 1.684 Net Concentration: 47.500 268.030 79.125 1.094 1.004

Phase 2

Sample: 47.914 119.395 51.466 0.673 2.176 Ambient: 4.749 0.000 0.072 0.043 1.694 Net Concentration: 43.409 119.395 51.398 0.632 0.570

Phase 3

Sample: 44.412 179.113 80.364 0.983 1.980 Ambient: 4.854 0.000 0.104 0.043 1.692 Net Concentration: 39.923 179.113 80.268 0.943 0.415

Mass Results (g/ km)/(g)

Phase 1 0.331 1.909 3.835 22.114 1.898 10.945 Phase 2 0.491 3.025 2.723 16.781 1.962 12.094 Phase 3 0.282 1.626 2.548 14.691 1.901 10.964 Weighted (Phase1,2,3) 0.400 2.906 1.932

Mass Results (g/ km)/(g)

Phase 1 246.191 1,419.689 0.008 0.047 0.330 1.901 Phase 2 226.727 1,397.525 0.007 0.046 0.484 2.984 Phase 3 210.947 1,216.343 0.003 0.019 0.279 1.606 Weighted (Phase1,2,3) 226.425 0.006 0.395

Fuel Economy (km/liter)

Phase 1 10.403

Phase 2 11.330

Phase 3 12.207

THC

CO

Nox

REPRODUÇÕES DESTE DOCUMENTO SÓ TÊM VALIDADE SE FOREM INTEGRAIS E AUTORIZADAS PELO LACTEC

DOC LEME - 31 Data: AGO/2010 Revisão: 05

Run Number: 8453 Requester: ECOFUEL

Test Cell: LACTEC LEME Vehicle Type: S-10

Test Date: 07-Dec-2011 Vehicle ID: 9BG138JJ0B0431489

Test Start Time: 00:17:35 Transmission: Manual

Test Type: Brazil Cert Odometer: (km) 34981

Operador: CARLOS Inertia Wt: (kg) 2041

Driver: CARLOS Dyno Coeff A: (nt) 307.02

Fuel Type: Diesel_S10_01_11 Dyno Coeff B: (nt/kph) 0.0000

Shift Table 1: 15_30_48_70 Dyno Coeff C: (nt/kph^2) 0.062803

Shift Table 2: 3PH_15_30_48_70 Dyno hp @ 50 mph: 21.4

Soak Start Date: 06/12/2011 Driver Errors: 0

Soak Start Time: 06:10 Pretest Remarks:

Test Conditions

Phase 1

Phase 2

Phase 3

Phase Start Time(hh:mm:ss): 00:24:54 00:33:20 00:57:37

Particulate Flow Time(sec): 506.0 866.7 506.1

Avg. CVS Flow Rate(m^3/min): 8.35 8.31 8.29

CVS Volume (m^3 20degC): 70.80 120.61 70.38

CVS Dilution factor: 11.494 19.423 13.331

Distance(km): 5.767 6.164 5.766

Crank Time(sec): 0.9 - 1.0

Hold Time(sec): 0.0 0.0 0.0

Avg. Cell Temp.(degC): 22.2 22.4 22.6

Avg. Barometer(kPa): 91.23 91.23 91.22

Avg. Dew Point(degC): 14.32 14.26 14.04

Avg. Specific Humidity(gm/kg): 11.31 11.27 11.11

Avg. Relative Humidity(%): 60.8 60.0 58.5

Particulate Conditions

Avg. Particulate Flow Rate(L/min): 29.7 30.1 29.8

Particulate Volume(L): 250.4 435.4 251.8

Avg. Particulate Temp.(degC): 23.7 24.1 24.7

Avg. Tunnel Temp.(degC): 32.4 34.9 34.7

Sample Particulate Filters

Filter Number

1

2

3

Init. Primary Filter Mass(mg) 70.919 77.675 68.992

Final Primary Filter Mass(mg) 73.926 78.960 71.043

Initial Secondary Filter Mass(mg) 67.426 71.402 72.028

Final Secondary Filter Mass(mg) 67.482 71.547 72.135

Net Combined Filter Mass(mg) 3.0070 1.4300 2.0510

Particulate Results

Filter Mass (g) 0.8491 0.3957 0.5726

Particulate Mass (g/km) 0.1473 0.0642 0.0993

Weighted Particulate Mass

Run Number: 8468 Requester: ECOFUEL

Test Cell: LACTEC LEME Vehicle Type: S-10

Test Date: 08-Dec-2011 Vehicle ID: 9BG138JJ0B0431489

Test Start Time: 00:41:57 Transmission: Manual

Test Type: Brazil Cert Odometer: (km) 35012

Operador: CARLOS Inertia Wt: (kg) 2041

Driver: CARLOS Dyno Coeff A: (nt) 307.02

Fuel Type: Diesel_S10_01_11 Dyno Coeff B: (nt/kph) 0.0000

Shift Table 1: 15_30_48_70 Dyno Coeff C: (nt/kph^2) 0.062803

Shift Table 2: 3PH_15_30_48_70 Dyno hp @ 50 mph: 21.4

Soak Start Date: 07/12/2011 Driver Errors: 0

Soak Start Time: 11:56 Pretest Remarks: Com Aditivo

Test Conditions

Phase 1

Phase 2

Phase 3

Phase Start Time: 00:47:53 00:56:19 01:20:36

Test Time (sec): 506.0 866.8 506.1

Avg. CVS Flow Rate (m^3/min) 8.33 8.29 8.28

CVS Volume (m^3 20degC) 70.62 120.35 70.23

Dilution factor: 11.724 19.418 13.347

Bag Analysis Time (sec): 1011.8 272.2 184.6

Driver Out of Limits (sec): 0.0 0.0 0.0

Distance (km) 5.739 6.158 5.769

Crank Time (sec): 0.7 - 1.0

Hold Time (sec): 0.0 0.0 0.0

Avg. Cell Temp (degC) 23.1 22.6 22.9

Avg. Barometer (kPa) 91.09 91.09 91.08

Avg Dew Point (degC) 15.08 14.79 15.08

Avg. Real Humidity (%) 60.5 61.3 61.3

Specific Humidity (gm/kg) 11.91 11.68 11.91

Hum Corr Factor: 1.041 1.033 1.041

Bag Results

THC

CO

NOx

CO2

CH4

Phase 1

(ppm)

(ppm)

(ppm)

(%)

(ppm)

Sample: 47.840 255.446 77.555 1.113 2.228 Ambient: 4.001 1.716 0.142 0.043 1.569 Net Concentration: 44.180 253.877 77.425 1.073 0.793

Phase 2

Sample: 48.007 123.289 51.392 0.673 2.046 Ambient: 4.952 1.562 0.113 0.043 1.570 Net Concentration: 43.310 121.808 51.285 0.632 0.557

Phase 3

Sample: 45.418 174.454 79.491 0.982 1.845 Ambient: 5.208 1.621 0.108 0.043 1.568 Net Concentration: 40.600 172.955 79.391 0.942 0.394

Mass Results (g/ km)/(g)

Phase 1 0.308 1.766 3.641 20.895 1.900 10.904 Phase 2 0.489 3.009 2.774 17.084 1.983 12.211 Phase 3 0.287 1.654 2.454 14.156 1.927 11.118 Weighted (Phase1,2,3) 0.395 2.866 1.950

Mass Results (g/ km)/(g)

Phase 1 241.993 1,388.872 0.007 0.037 0.308 1.770 Phase 2 226.475 1,394.675 0.007 0.045 0.483 2.972 Phase 3 210.186 1,212.592 0.003 0.018 0.283 1.631 Weighted (Phase1,2,3) 225.203 0.006 0.391

Fuel Economy (km/liter)

Phase 1 10.595

Phase 2 11.338

Phase 3 12.258

THC

CO

Nox

REPRODUÇÕES DESTE DOCUMENTO SÓ TÊM VALIDADE SE FOREM INTEGRAIS E AUTORIZADAS PELO LACTEC

DOC LEME - 31 Data: AGO/2010 Revisão: 05

Run Number: 8468 Requester: ECOFUEL

Test Cell: LACTEC LEME Vehicle Type: S-10

Test Date: 08-Dec-2011 Vehicle ID: 9BG138JJ0B0431489

Test Start Time: 00:41:57 Transmission: Manual

Test Type: Brazil Cert Odometer: (km) 35012

Operador: CARLOS Inertia Wt: (kg) 2041

Driver: CARLOS Dyno Coeff A: (nt) 307.02

Fuel Type: Diesel_S10_01_11 Dyno Coeff B: (nt/kph) 0.0000

Shift Table 1: 15_30_48_70 Dyno Coeff C: (nt/kph^2) 0.062803

Shift Table 2: 3PH_15_30_48_70 Dyno hp @ 50 mph: 21.4

Soak Start Date: 07/12/2011 Driver Errors: 0

Soak Start Time: 11:56 Pretest Remarks: Com Aditivo

Test Conditions

Phase 1

Phase 2

Phase 3

Phase Start Time(hh:mm:ss): 00:47:53 00:56:19 01:20:36

Particulate Flow Time(sec): 506.0 866.8 506.1

Avg. CVS Flow Rate(m^3/min): 8.33 8.29 8.28

CVS Volume (m^3 20degC): 70.62 120.35 70.23

CVS Dilution factor: 11.724 19.418 13.347

Distance(km): 5.739 6.158 5.769

Crank Time(sec): 0.7 - 1.0

Hold Time(sec): 0.0 0.0 0.0

Avg. Cell Temp.(degC): 23.1 22.6 22.9

Avg. Barometer(kPa): 91.09 91.09 91.08

Avg. Dew Point(degC): 15.08 14.79 15.08

Avg. Specific Humidity(gm/kg): 11.91 11.68 11.91

Avg. Relative Humidity(%): 60.5 61.3 61.3

Particulate Conditions

Avg. Particulate Flow Rate(L/min): 29.7 30.1 29.9

Particulate Volume(L): 250.8 435.8 252.2

Avg. Particulate Temp.(degC): 24.2 24.8 25.0

Avg. Tunnel Temp.(degC): 32.1 35.1 34.8

Sample Particulate Filters

Filter Number

1

2

3

Init. Primary Filter Mass(mg) 70.337 72.176 70.496

Final Primary Filter Mass(mg) 73.022 73.495 72.457

Initial Secondary Filter Mass(mg) 71.483 68.531 69.876

Final Secondary Filter Mass(mg) 71.613 68.718 69.966

Net Combined Filter Mass(mg) 2.6850 1.5060 1.9610

Particulate Results

Filter Mass (g) 0.7553 0.4155 0.5456

Particulate Mass (g/km) 0.1316 0.0675 0.0946

Weighted Particulate Mass

Run Number: 8537 Requester: ECOFUEL

Test Cell: LACTEC LEME Vehicle Type: VW AMAROK

Test Date: 14-Dec-2011 Vehicle ID: WV1DD42H8CA006522

Test Start Time: 05:18:26 Transmission: MANUAL

Test Type: Brazil Cert Odometer: (km) 124

Operador: CARLOS Inertia Wt: (kg) 2155

Driver: CARLOS Dyno Coeff A: (nt) 234.20

Fuel Type: Diesel_S10_01_11 Dyno Coeff B: (nt/kph) 0.0000

Shift Table 1: 25_40_65_72 Dyno Coeff C: (nt/kph^2) 0.064900

Shift Table 2: EPA505_5spd_25_40_65_72 Dyno hp @ 50 mph: 19.6

Soak Start Date: 13/12/2011 Driver Errors: 0

Soak Start Time: 04:00 Pretest Remarks:

Test Conditions

Phase 1

Phase 2

Phase 3

Phase Start Time: 05:23:47 05:32:13 05:57:00

Test Time (sec): 506.0 866.9 505.9

Avg. CVS Flow Rate (m^3/min) 8.24 8.22 8.22

CVS Volume (m^3 20degC) 69.83 119.36 69.77

Dilution factor: 12.211 18.701 13.704

Bag Analysis Time (sec): 1011.5 271.3 184.1

Driver Out of Limits (sec): 0.0 0.0 0.0

Distance (km) 5.785 6.162 5.754

Crank Time (sec): 0.7 - 0.7

Hold Time (sec): 0.0 0.0 0.0

Avg. Cell Temp (degC) 23.4 23.2 23.2

Avg. Barometer (kPa) 90.76 90.72 90.69

Avg Dew Point (degC) 13.89 13.69 13.72

Avg. Real Humidity (%) 55.1 54.9 55.2

Specific Humidity (gm/kg) 11.05 10.91 10.94

Hum Corr Factor: 1.011 1.007 1.008

Bag Results

THC

CO

NOx

CO2

CH4

Phase 1

(ppm)

(ppm)

(ppm)

(%)

(ppm)

Sample: 11.753 19.587 29.180 1.094 2.468 Ambient: 3.507 1.156 0.051 0.042 1.793 Net Concentration: 8.533 18.525 29.133 1.055 0.822

Phase 2

Sample: 8.397 2.714 18.376 0.715 2.390 Ambient: 3.379 2.126 0.042 0.042 1.811 Net Concentration: 5.198 0.701 18.336 0.675 0.676

Phase 3

Sample: 7.822 2.373 39.166 0.977 2.099 Ambient: 3.411 1.791 0.075 0.043 1.796 Net Concentration: 4.660 0.713 39.097 0.937 0.434

Mass Results (g/ km)/(g)

Phase 1 0.060 0.345 0.261 1.508 0.681 3.941 Phase 2 0.057 0.353 0.016 0.098 0.685 4.220 Phase 3 0.032 0.186 0.010 0.058 0.915 5.264 Weighted (Phase1,2,3) 0.051 0.065 0.747

Mass Results (g/ km)/(g)

Phase 1 233.406 1,350.216 0.007 0.038 0.054 0.311 Phase 2 239.700 1,476.935 0.009 0.054 0.051 0.312 Phase 3 208.270 1,198.332 0.004 0.020 0.030 0.170 Weighted (Phase1,2,3) 229.738 0.007 0.046

Fuel Economy (km/liter)

Phase 1 11.260

Phase 2 10.983

Phase 3 12.644

THC

CO

Nox

REPRODUÇÕES DESTE DOCUMENTO SÓ TÊM VALIDADE SE FOREM INTEGRAIS E AUTORIZADAS PELO LACTEC

DOC LEME - 31 Data: AGO/2010 Revisão: 05

Run Number: 8537 Requester: ECOFUEL

Test Cell: LACTEC LEME Vehicle Type: VW AMAROK

Test Date: 14-Dec-2011 Vehicle ID: WV1DD42H8CA006522

Test Start Time: 05:18:26 Transmission: MANUAL

Test Type: Brazil Cert Odometer: (km) 124

Operador: CARLOS Inertia Wt: (kg) 2155

Driver: CARLOS Dyno Coeff A: (nt) 234.20

Fuel Type: Diesel_S10_01_11 Dyno Coeff B: (nt/kph) 0.0000

Shift Table 1: 25_40_65_72 Dyno Coeff C: (nt/kph^2) 0.064900

Shift Table 2: EPA505_5spd_25_40_65_72 Dyno hp @ 50 mph: 19.6

Soak Start Date: 13/12/2011 Driver Errors: 0

Soak Start Time: 04:00 Pretest Remarks:

Test Conditions

Phase 1

Phase 2

Phase 3

Phase Start Time(hh:mm:ss): 05:23:47 05:32:13 05:57:00

Particulate Flow Time(sec): 506.0 866.9 505.9

Avg. CVS Flow Rate(m^3/min): 8.24 8.22 8.22

CVS Volume (m^3 20degC): 69.83 119.36 69.77

CVS Dilution factor: 12.211 18.701 13.704

Distance(km): 5.785 6.162 5.754

Crank Time(sec): 0.7 - 0.7

Hold Time(sec): 0.0 0.0 0.0

Avg. Cell Temp.(degC): 23.4 23.2 23.2

Avg. Barometer(kPa): 90.76 90.72 90.69

Avg. Dew Point(degC): 13.89 13.69 13.72

Avg. Specific Humidity(gm/kg): 11.05 10.91 10.94

Avg. Relative Humidity(%): 55.1 54.9 55.2

Particulate Conditions

Avg. Particulate Flow Rate(L/min): 29.8 29.7 29.8

Particulate Volume(L): 251.1 429.4 251.9

Avg. Particulate Temp.(degC): 25.5 25.8 26.1

Avg. Tunnel Temp.(degC): 33.8 34.9 34.9

Sample Particulate Filters

Filter Number

1

2

3

Init. Primary Filter Mass(mg) 66.391 61.107 62.456

Final Primary Filter Mass(mg) 67.450 62.205 63.181

Initial Secondary Filter Mass(mg) 64.453 62.954 65.735

Final Secondary Filter Mass(mg) 64.482 62.991 65.761

Net Combined Filter Mass(mg) 1.0590 1.0980 0.7250

Particulate Results

Filter Mass (g) 0.2942 0.3049 0.2005

Particulate Mass (g/km) 0.0509 0.0495 0.0349

Weighted Particulate Mass

Run Number: 8556 Requester: ECOFUEL

Test Cell: LACTEC LEME Vehicle Type: VW AMAROK

Test Date: 15-Dec-2011 Vehicle ID: WV1DD42H8CA006522

Test Start Time: 06:22:33 Transmission: MANUAL

Test Type: Brazil Cert Odometer: (km) 154

Operador: CARLOS Inertia Wt: (kg) 2155

Driver: CARLOS Dyno Coeff A: (nt) 234.20

Fuel Type: Diesel_S10_01_11 Dyno Coeff B: (nt/kph) 0.0000

Shift Table 1: 25_40_65_72 Dyno Coeff C: (nt/kph^2) 0.064900

Shift Table 2: EPA505_5spd_25_40_65_72 Dyno hp @ 50 mph: 19.6

Soak Start Date: 14/12/2011 Driver Errors: 0

Soak Start Time: 10:58 Pretest Remarks: Com Aditivo

Test Conditions

Phase 1

Phase 2

Phase 3

Phase Start Time: 06:27:51 06:36:17 07:00:34

Test Time (sec): 505.9 866.4 505.9

Avg. CVS Flow Rate (m^3/min) 8.26 8.23 8.22

CVS Volume (m^3 20degC) 70.06 119.47 69.73

Dilution factor: 12.049 18.669 13.713

Bag Analysis Time (sec): 1011.4 271.7 184.5

Driver Out of Limits (sec): 0.0 0.0 0.0

Distance (km) 5.758 6.111 5.719

Crank Time (sec): 0.8 - 0.8

Hold Time (sec): 0.0 0.0 0.0

Avg. Cell Temp (degC) 23.3 23.2 23.5

Avg. Barometer (kPa) 90.48 90.48 90.49

Avg Dew Point (degC) 14.42 14.05 14.32

Avg. Real Humidity (%) 57.3 56.4 56.5

Specific Humidity (gm/kg) 11.48 11.21 11.40

Hum Corr Factor: 1.026 1.017 1.023

Bag Results

THC

CO

NOx

CO2

CH4

Phase 1

(ppm)

(ppm)

(ppm)

(%)

(ppm)

Sample: 10.634 13.964 23.996 1.110 2.457 Ambient: 2.845 0.041 0.025 0.047 1.791 Net Concentration: 8.025 13.926 23.973 1.067 0.815

Phase 2

Sample: 8.366 1.225 17.906 0.717 2.396 Ambient: 2.868 0.001 0.022 0.046 1.804 Net Concentration: 5.652 1.224 17.885 0.673 0.689

Phase 3

Sample: 7.853 1.394 39.194 0.976 2.115 Ambient: 2.999 0.239 0.104 0.046 1.795 Net Concentration: 5.073 1.173 39.098 0.934 0.451

Mass Results (g/ km)/(g)

Phase 1 0.056 0.321 0.197 1.137 0.573 3.301 Phase 2 0.063 0.385 0.028 0.170 0.681 4.161 Phase 3 0.036 0.207 0.017 0.095 0.934 5.343 Weighted (Phase1,2,3) 0.054 0.060 0.728

Mass Results (g/ km)/(g)

Phase 1 237.838 1,369.578 0.007 0.038 0.051 0.292 Phase 2 241.026 1,472.840 0.009 0.055 0.056 0.343 Phase 3 208.637 1,193.094 0.004 0.021 0.033 0.186 Weighted (Phase1,2,3) 231.436 0.007 0.048

Fuel Economy (km/liter)

Phase 1 11.056

THC

CO

Nox

REPRODUÇÕES DESTE DOCUMENTO SÓ TÊM VALIDADE SE FOREM INTEGRAIS E AUTORIZADAS PELO LACTEC

DOC LEME - 31 Data: AGO/2010 Revisão: 05

Run Number: 8556 Requester: ECOFUEL

Test Cell: LACTEC LEME Vehicle Type: VW AMAROK

Test Date: 15-Dec-2011 Vehicle ID: WV1DD42H8CA006522

Test Start Time: 06:22:33 Transmission: MANUAL

Test Type: Brazil Cert Odometer: (km) 154

Operador: CARLOS Inertia Wt: (kg) 2155

Driver: CARLOS Dyno Coeff A: (nt) 234.20

Fuel Type: Diesel_S10_01_11 Dyno Coeff B: (nt/kph) 0.0000

Shift Table 1: 25_40_65_72 Dyno Coeff C: (nt/kph^2) 0.064900

Shift Table 2: EPA505_5spd_25_40_65_72 Dyno hp @ 50 mph: 19.6

Soak Start Date: 14/12/2011 Driver Errors: 0

Soak Start Time: 10:58 Com Aditivo

Test Conditions

Phase 1

Phase 2

Phase 3

Phase Start Time(hh:mm:ss): 06:27:51 06:36:17 07:00:34

Particulate Flow Time(sec): 505.9 866.4 505.9

Avg. CVS Flow Rate(m^3/min): 8.26 8.23 8.22

CVS Volume (m^3 20degC): 70.06 119.47 69.73

CVS Dilution factor: 12.049 18.669 13.713

Distance(km): 5.758 6.111 5.719

Crank Time(sec): 0.8 - 0.8

Hold Time(sec): 0.0 0.0 0.0

Avg. Cell Temp.(degC): 23.3 23.2 23.5

Avg. Barometer(kPa): 90.48 90.48 90.49

Avg. Dew Point(degC): 14.42 14.05 14.32

Avg. Specific Humidity(gm/kg): 11.48 11.21 11.40

Avg. Relative Humidity(%): 57.3 56.4 56.5

Particulate Conditions

Avg. Particulate Flow Rate(L/min): 29.8 29.7 29.9

Particulate Volume(L): 251.1 429.1 252.3

Avg. Particulate Temp.(degC): 25.3 25.6 25.9

Avg. Tunnel Temp.(degC): 32.7 34.4 35.0

Sample Particulate Filters

Filter Number

1

2

3

Init. Primary Filter Mass(mg) 64.748 57.961 66.158

Final Primary Filter Mass(mg) 65.716 59.088 66.916

Initial Secondary Filter Mass(mg) 58.702 61.106 59.892

Final Secondary Filter Mass(mg) 58.735 61.140 59.921

Net Combined Filter Mass(mg) 0.9680 1.1270 0.7580

Particulate Results

Filter Mass (g) 0.2698 0.3134 0.2093

Particulate Mass (g/km) 0.0469 0.0513 0.0366

Weighted Particulate Mass