Solidification Furnace for Microgravity Experiments on
Sounding Rockets
Chen Ying An*, Cesar Boschetti, Manuel Francisco Ribeiro, Rafael Cardoso Toledo, Filipe Estevão Freitas, Felipe Fernandes Castilho, Iraja Newton Bandeira
Instituto Nacional de Pesquisas Espaciais – São José dos Campos/SP – Brazil
Abstract: The Brazilian Microgravity Program is mainly based on experiments carried out on sounding rockets. Up to present days, three missions carrying a total of experiments were made. ,n all Àights, a fast solidi¿cation furnace, capable of producing temperatures up to 900º C, was used to process metal and semiconductor alloys in microgravity environment. This paper has described the furnace and the solidi¿cation experiment made during the last parabolic Àight, called Maracati Mission, which has occurred in 'ecember, 00.
Keywords: Microgravity, 6uborbital Àights, 6olidi¿cation furnace, $lloys solidi¿cation.
INTRODUCTION
The Brazilian Microgravity Program, which is supported by the Brazilian Space Agency (AEB), selects microgravity exper-LPHQWVSURYLGLQJSDUWLDO¿QDQFLDOVXSSRUWIRUWKHDSSURYHG SURMHFWVVLQFHWKHLULQLWLDOGHVLJQSKDVHVXSWRWKHÀLJKWPLVVLRQ
The Microgravity Program has contemplated missions on the International Space Station (ISS) in 2006 (Bandei-UDHWDODQGRQWKH%UD]LOLDQPDGHVRXQGLQJURFNHWV &RUUrDHWDO7KH¿UVWSDUDEROLFÀLJKWZDVLQ and eight microgravity experiments were selected by the First $QQRXQFHPHQWRI2SSRUWXQLW\$2RIWKHSURJUDPLQDUHDV VXFKDV%LRORJ\0DWHULDO6FLHQFHVDQG7UDQVSRUW3KHQRPHQD 7KHH[SHULPHQWVZHUHODXQFKHGIURPWKH%UD]LOLDQ$OFkQWD-ra Launching Center (CLA), onboard an one-stage B7KHH[SHULPHQWVZHUHODXQFKHGIURPWKH%UD]LOLDQ$OFkQWD-razilian 96VRXQGLQJURFNHWWKUHHWRIRXUPLQXWHVRIPLFURJUDYLW\ PDGHE\WKH,QVWLWXWHRI$HURQDXWLFVDQG6SDFH,$(IURPWKH $HURVSDFH7HFKQRORJ\DQG6FLHQFH'HSDUWPHQW'&7$ $VHFRQGÀLJKWZDVGRQHLQDQGDWKLUGLQZLWK DPRUHSRZHUIXOWZRVWDJHVRXQGLQJURFNHWZKLFKLVGHQRPL-QDWHG96%VL[WRHLJKWPLFURJUDYLW\PLQXWHV7KLVURFNHW LVFDSDEOHRIWUDQVSRUWLQJSD\ORDGVZLWKPDVVXSWRNJ GXULQJDERXWVHFRQGVLQDEDOOLVWLFÀLJKWDERYHNP $IWHUWKHSDUDEROLFÀLJKWLWIHOOLQWRWKHVHDDLGHGE\SDUDFKXWHV DQGZDVUHFRYHUHGE\WKH%UD]LOLDQ$LU)RUFHKHOLFRSWHUV
7KHSD\ORDGSODWIRUPXVHGWRFDUU\WKHH[SHULPHQWVZDV PDGHE\WKH*HUPDQ$HURVSDFH&HQWHU'/5025$%$LQ cooperation with IAE (Garcia et al.DQGLVVKRZQLQ )LJWRJHWKHUZLWKWKH96DQG96%URFNHWV
VS-30 VSB-30 Plataform
)LJXUH %UD]LOLDQVRXQGLQJURFNHWVDQGPLFURJUDYLW\SODWIRUP
SOLIDIFICATION FURNACE
$JURXSRIWKH%UD]LOLDQ6SDFH5HVHDUFK,QVWLWXWH,13( KDV SURSRVHG WR SURMHFW FRQVWUXFW DQG TXDOLI\ D FRPSDFW IXUQDFH DV D SHUPDQHQW IDFLOLW\ IRU WKH VRXQGLQJ URFNHWV microgravity program in order to be used by several groups GRLMDWP
5HFHLYHG$FFHSWHG DXWKRUIRUFRUUHVSRQGHQFHFKHQ#ODVLQSHEU $YHQLGDGRV$VWURQDXWDV±-DUGLPGD*UDQMD &(3±6mR-RVpGRV&DPSRV63±%UD]LO
WKDWZRUNHGLQWKDWDUHD%DQGHLUDet al.DQG7KH SXUSRVHRIWKHIXUQDFHLVWRPHOWDQGVROLGLI\PHWDOVDQGVHPL
-FRQGXFWRUDOOR\VZLWKIXVLRQSRLQWXSWR&7KHIXUQDFH VKRXOGEHFDSDEOHRIDIDVWFRROLQJFRPSDWLEOHZLWKWKHVKRUW PLFURJUDYLW\WLPHVRIVXERUELWDOÀLJKWVLQRUGHUWRVROLGLI\ VDPSOHVXSWRPPGLDPHWHUDQGXSWRPPOHQJWK 7KHWXEXODUIXUQDFHZDVKHDWHGDQGFRQWUROOHGIURPWKHJURXQG WKURXJKWKHURFNHWXPELOLFDOFDEOHXQWLOLWUHDFKHGWKHGHVLUHG WHPSHUDWXUH$IWHUODXQFKWKHWHPSHUDWXUHZDVNHSWE\WKHUPDO LQHUWLD$VVRRQDVWKHPLFURJUDYLW\HQYLURQPHQWZDVUHDFKHGD PRWRUGURYHWKHKRWSDUWRIWKHIXUQDFHWRDQXSSHUSRVLWLRQLQOHVV WKDQHLJKWVHFRQGVZKLOHWKHVDPSOHUHPDLQHG¿[HGDWWKHFROG UHJLRQDQGDIDVWFRROLQJZDVREWDLQHG)LJXUHVKRZVWKHIXUQDFH LQWKHWZRSRVLWLRQVGHVFULEHG$WWKHULJKWVLGHRIWKHIXUQDFHWKHUH LVWKHHOHFWURQLFVFRQWUROER[,WFRQWDLQVDGDWDORJJHUIRUWKHW\SH .WKHUPRFRXSOHVEDWWHULHVIRUWKHIXUQDFHGULYHPRWRUWLPHUIRU PRWRUVWRSSLQJDPSOL¿HUIRUWHOHPHWU\WHPSHUDWXUHVLJQDOVDQGWKH FLUFXLWIRUWKHFRQWUROWKHUPRFRXSOHDQGSRZHUFDEOHVFRQQHFWHGWR DFRQWUROOHUXQLWDQGD'&9VRXUFHZKLFKSRZHUVWKHIXUQDFH IURPWKHJURXQGSURYLGLQJDWHPSHUDWXUHVWDELOLW\RI&
)LJXUH 6ROLGL¿FDWLRQIXUQDFHLQLWVWZRZRUNLQJSKDVHVSRVLWLRQHG at the bottom, heating the sample during ground and ascend-LQJSHULRGDQGGLVORFDWHGWRWKHWRSSHUPLWWLQJDIDVWVDPSOH FRROLQJGXULQJPLFURJUDYLW\
The experiment temperature is monitored by thermocou-ples and their signals are stored in an internal data logger, as
ZHOODVVHQWWRJURXQGE\WHOHPHWU\
7KHH[SORGHGGUDZLQJRIWKHIXUQDFHLVVKRZQLQ)LJ,W FRPSULVHVDWXEXODUIXUQDFHPDGHRIVWDLQOHVVVWHHOZLWKPP RIGLDPHWHUDQGPPRIOHQJWK7KHSURFHVVLQJFKDPEHURIWKH
materials is a ceramic tube with 20 mm diameter, running through
WKHZKROHIXUQDFHOHQJWK7KHXSSHUPPSDUWRIWKHFHUDPLF
tube is evolved by a shielded electrical resistance, and quartz
¿EHULVHPSOR\HGDVWKHUPDOLQVXODWLRQ7KHUHPDLQLQJUHVLVWDQFH IUHHSRUWLRQSURGXFHVDWKHUPDOJUDGLHQWEHWZHHQWKHXSSHUKRW VHFWLRQDQGWKHFROGERWWRPRQHLQWKHRUGHURI&FP7KHUH LVDQH[WHUQDOVWUXFWXUHKROGLQJWKHIXUQDFHDOORZLQJDQXSDQG GRZQPRYHPHQWZLWKWKHDLGRIDQHOHFWULFPRWRU7KHVWUXFWXUH
also supports a stainless steel sample holder tube placed inside
WKHFHUDPLFFDYLW\7KHV\VWHPKDVDWRWDOGLDPHWHURIPP DQGDWRWDOOHQJWKRIPPZHLJKWLQJDURXQGNJ
)LJXUH ([SORGHG YLHZ RI WKH VROLGL¿FDWLRQ IXUQDFH IXUQDFH WRSRIWKHH[WHUQDOVWUXFWXUHGULYLQJPRWRUVDPSOH KROGHUMDFNVFUHZVWUXFWXUDOEDUVVOLGLQJJXLGHEDUV
THE MARACATI MISSION
,Q'HFHPEHUD96%URFNHWGHSDUWHGIURPWKH &/$FDUU\LQJWHQPLFURJUDYLW\H[SHULPHQWVIURP%UD]LOLDQ XQLYHUVLWLHVDQGUHVHDUFKFHQWHUV7KHDSRJHHZDVNPDQG WKHWRWDOÀLJKWWLPHZDVPLQXWHVIURPZKLFKVL[PLQXWHV ZHUH LQ PLFURJUDYLW\7KH SD\ORDG IHOO RQ WKH VHD DQG ZDV UHVFXHGDERXWRQHKRXUODWHU7KHH[SHULPHQWVLQFOXGHGWKH VROLGL¿FDWLRQIXUQDFHGHVFULEHGPDGHDWWKH6HQVRUVDQG0DWH -rials Associate Laboratory (LAS), at INPE (An et al. ,Q WKLV IOLJKW D VROLGLILFDWLRQ H[SHULPHQW ZLWK WZR HXWHFWLF DOOR\V ZDV FDUULHG RXW 7KH HXWHFWLF FRPSRVLWLRQ 3EDWRIWKH3E7HDOOR\ZLWKDIXVLRQSRLQWRI& DQGWKHHXWHFWLFFRPSRVLWLRQ3EDWRIWKH3E6QDOOR\ IXVLRQSRLQWRI&ZHUHXVHG
(DFKVDPSOHZLWKJPDVVZDVVHDOHGXQGHUYDFXXP
$Q&<et al
ZLWKLQ D TXDUW] DPSRXOH ZLWK PP OHQJWK DQG PP GLDPHWHUVKRZQLQ)LJ
)LJXUH (XWHFWLF3ETe (top) and PbSnDPSRXOHVDIWHU WKHPLFURJUDYLW\ÀLJKW
7KHDPSRXOHVZHUH¿WWHGLQVLGHWKHVWDLQOHVVVWHHOWXEH VDPSOHKROGHUDQGWKHIXUQDFHZDVKHDWHGLQWKHJURXQGWRD VHWSRLQWRI&XVLQJWKHURFNHWXPELOLFDOFDEOHPLQXWHV EHIRUHODXQFK7KHVDPSOHWHPSHUDWXUHVZHUHPRQLWRUHGE\ the on-board data logger as well as by telemetry, and the IXUQDFHWHPSHUDWXUHJUDGLHQWLVVKRZQLQ)LJ
)LJXUH 7HPSHUDWXUH JUDGLHQW RI WKH VROLGLILFDWLRQ IXUQDFH VKRZLQJ WKH SRVLWLRQ RI WKH VDPSOHV TXDUW] DPSRXOHV LQVLGHWKHVDPSOHKROGHU
7KHPLFURJUDYLW\OHYHODWWDLQHGZDVLQWKHRUGHURIg, which ZDVHQRXJKWRFDXVHSUHGRPLQDQFHRI0DUDQJRQLFRQYHFWLRQ over the thermal and constitutional gravitational dependent FRQYHFWLRQVZKLFKZLOODOORZWKHVWXG\RIWKHVXSHU¿FLDOWHQVLRQ LQÀXHQFHLQWKH3E7HDQG3E6QHXWHFWLFDOOR\V
$OOODXQFKLQJSURFHGXUHVDQGÀLJKWSKDVHVRFFXUUHGDV SODQQHG:KHQWKHURFNHWZDVODXQFKHGWKHIXUQDFHSRZHU ZDVVZLWFKHGRII7KHWZRVWDJHURFNHWZRUNHGQRPLQDOO\ DQGWKHSD\ORDGUHDFKHGPLFURJUDYLW\DERXWRQHPLQXWHDIWHU
ODXQFKLQJ$VWKHDFFHOHUDWLRQVHQVRUGHWHFWHGWKHPLFURJUDY-LW\SURSHUOHYHOLWVHQWDVLJQDOWRWKHIXUQDFHDQGWKHKHDWHU SDUWZDVPRYHGWRWKHWRSRIWKHV\VWHPLQHLJKWVHFRQGVOHDY-LQJWKHVDPSOHVIUHHWRFRROGRZQ
$IWHUVL[PLQXWHVWKHSD\ORDGVWDUWHGWKHUHHQWU\WUDMHF-WRU\7KHSDUDFKXWHVZHUHRSHQHGDWWKHSURSHUDOWLWXGHWKH SD\ORDGIHOODQGÀRDWHGLQWKHVHDDQGZDVODWHUUHFRYHUHGE\ D%UD]LOLDQ$LU)RUFH)$%GLYLQJWHDP
7KHF\FOHEHKDYLRUZDVDVH[SHFWHGWKHIXUQDFHWHPSHUDWXUH KDGDVPDOOGURSRIDERXW&GXULQJWKHURFNHWDVFHQGLQJGXH WRRQHPLQXWHZLWKRXWSRZHU5HDFKLQJPLFURJUDYLW\DVVRRQ DVWKHIXUQDFHPRYHGWRWKHXSSHUSRVLWLRQDIWHUVHFRQGV WKHWHPSHUDWXUHGURSZDVRI&IRUWKH3E7HDOOR\DQG& IRUWKH3E6QDOOR\DOORZLQJWKHIDVWFRROLQJQHHGHGIRUERWK eutectic PbTe and PbSnVROLGL¿FDWLRQH[SHULPHQWV 7KHWHOHPHWU\GDWDIRUWKHIXUQDFHWKHUPDOF\FOHDUHVKRZQ LQ)LJIRUERWKVDPSOHV
)LJXUH 7HOHPHWU\GDWDRIWKHVROLGL¿FDWLRQIXUQDFHWKHUPDOF\FOH GXULQJWKHPLFURJUDYLW\ÀLJKW
PRELIMINARY EXPERIMENT ANALYSIS
The samples have been analyzed and compared with others VROLGL¿HGDWJURXQGXVLQJWHFKQLTXHVVXFKDVGHQVLW\;UD\ GLIIUDFWLRQ;5'VFDQQLQJHOHFWURQPLFURVFRS\DQG;UD\ GLVSHUVLYHHQHUJ\VSHFWURVFRS\('6
,QRUGHUWRFRPSDUHWKHPLFURJUDYLW\VROLGL¿FDWLRQZLWKD normal gravity one, similar samples have been processed in laboratory with the same thermal gradient, which was shown LQ)LJDQGWKHUPDOF\FOH7KHIXUQDFHDQGLWVFRQWUROZHUH WKHVDPHXVHGRQWKHÀLJKWLWVHOI)LJDQG)LJFRPSDUHV WKHWKHUPDOF\FOHVXVHGWRVROLGLI\WKH3E7HDQG3E6QHXWHFWLF VDPSOHV RQ WKH ÀLJKW DQG RQ WKH ODERUDWRU\ 7KH VDPSOHV VROLGL¿HGDWWKHODERUDWRU\DUHSUHVHQWHGLQ)LJ
6ROLGL¿FDWLRQ)XUQDFHIRU0LFURJUDYLW\([SHULPHQWVRQ6RXQGLQJ5RFNHWV
Figure 7./DERUDWRU\H[SHULPHQWDOVHWXS
Figure 8.7KHUPDOF\FOHFXUYHVIRUWKHPLFURJUDYLW\ÀLJKWDQGWKH ODERUDWRU\H[SHULPHQW
Figure 9. (XWHFWLF 3E6Q DQG 3E7H VDPSOHV VROLGL¿HG LQ TXDUW] DPSRXOHVXQGHUQRUPDOJUDYLW\
CONCLUSIONS
7KH VROLGL¿FDWLRQ IXUQDFH SURYLGHG E\ /$6/INPE to
WKH %UD]LOLDQ VRXQGLQJ URFNHW SURJUDP LV TXDOL¿HG DQG
ready to be used by other groups that are interested in
PHOWLQJDQGVROLGLI\LQJDOOR\VLQJURXQGDQGLQPLFURJUDYLW\ HQYLURQPHQWV7KHIXUQDFHSUHVHQWVDQDSSURSULDWHWKHUPDO
mass to achieve rapid cooling time by conduction and
UDGLDWLRQ FRQVLVWHQW ZLWK WKH VKRUW ÀLJKW GXUDWLRQ DQG LWV HOHFWURQLF DQG PHFKDQLFDO FRPSRQHQWV SHUIRUPHG ZLWK SUHFLVLRQDQGUHOLDELOLW\GXULQJDOOPLVVLRQVWDJHV$VIRUWKH VFLHQWL¿F¿QGLQJVFRPSDULQJWKHDOOR\VJURZQLQPLFURJUDYLW\ DQGQRUPDOJUDYLW\WKHUHVXOWVZLOOEHSXEOLVKHGHOVHZKHUH
ACKNOWLEDGEMENTS
7KHDXWKRUVDUHWKDQNIXOWRWKH%UD]LOLDQ6SDFH$JHQF\$(% IRUVXSSRUWLQJWKHSUHVHQWSURMHFW
REFERENCES
$Q&<et al.³3HUIRUPDQFHRID6ROLGL¿FDWLRQ)XUQDFH 'HYHORSHGIRU6RXQGLQJ5RFNHWV´0LFURJUDYLW\6FLHQFHDQG 7HFKQRORJ\9RO1RSS
%DQGHLUD,1et al.³&HQWHQDU\0LVVLRQ)LUVW%UD]LOLDQ 0LFURJUDYLW\([SHULPHQWVDW,66´0LFURJUDYLW\6FLHQFHDQG 7HFKQRORJ\9RO1RSS
%DQGHLUD,1et al.DQG³)RUQR0XOWLXVXiULR SDUD6ROLGL¿FDomR5HVXOWDGRGDV0LVV}HV±2SHUDomR&XPm, H2SHUDomR&XPm,,´5HWULHYHGLQIURP
http://ZZZDHEJRYEUPLQLSKS"VHFDR PLFURJUDYLGDGH
&RUUrD )et al. ³%UD]LOLDQ 0LFURJUDYLW\ 3URJUDP &KDOOHQJHVDQG3HUVSHFWLYHV´3URFHHGLQJVRIWKHWK(6$ 6\PSRVLXPRQ(XURSHDQ5RFNHWDQG%DOORRQ3URJUDPPHV DQG 5HODWHG 5HVHDUFK 1RUZD\ 5HWULHYHG LQ IURP
http://DGVDEVKDUYDUGHGXDEV(6$63'
*DUFLD$et al.³96%6RXQGLQJ5RFNHW+LVWRU\RI )OLJKW3HUIRUPDQFH´-RXUQDORI$HURVSDFH7HFKQRORJ\DQG 0DQDJHPHQW9RO1RSS
$Q&<et al